Lab Report

Using english to report,
Purpose

·         To synthesize an ester out of an alcohol and a carboxylic acid.

Introduction


Everything that has scent is made up of molecules. Their scent is determined by the functional group each molecule contains, which is connected to an organic compound, a carbon-based molecule. These functional groups can determine whether a molecule is an alcohol, if it smells putrid (a carboxylic acid), or if it smells sweet (an ester). However, there are more than just three functional groups. When different functional groups react with one another, a new functional group is formed. For example, if an alcohol reacts with a carboxylic acid, an ester is formed. For this lab, this is exactly what we had to do. The class was assigned to combine alcohols and carboxylic acids in order to create different type of esters. If reacted correctly, the different properties of the different alcohols and carboxylic acids could make scents such as apple, strawberry, and banana.




Materials


·   Various Alcohols
·   Various Organic Acids
·   Test Tubes (5-8)
·   Hot Plate
·   Gloves
·   Goggles
·   Pipettes
·   Stirring Rods


Procedure


Wintergreen:

1.        Put 0.2 grams of salicylic acid into a 10 cm test tube.
2.        Add 6 drops of methyl alcohol add shake the tube until mixed.
3.        Add 1 drop of concentrated sulfuric acid.
4.        Shake the tube again and place it in a beaker of boiling water for three minutes.
5.        After heating is complete, remove the tube from beaker and add 15 drops of water.
6.        Hold the ester away from your face and waft the scent towards you.

Grape:

1.       Place 0.2 grams of anthranilic acid into a 10-cm test tube.
2.       Add 6 drops of methyl alcohol and agitate the tube until the contents are well mixed.
3.       Add 1 drop of concentrated sulfuric acid.
4.       Shake the tube and place it in a beaker of boiling water for three minutes.
5.       After heating is complete, remove the tube from breaker and add 15 drops of water.
6.       Hold the ester away from your face and waft the scent towards you.

Banana

1.       Put 6 drops of isoamyl alcohol in a 10-cm test tube.
2.       Add 2 drops of glacial acetic acid.
3.       Add 1 drop of concentrated sulfuric acid.
4.       Shake the tube and place it into boiling water.


5.       Remove the test tube from boiling water and add 20 drops of water. Shake tube.
6.       Wave the vapor of the scent towards you.

Strawberry:

1.       Put 6 drops of ethyl alcohol into a 10-cm test tube.
2.       Wearing gloves, add 2 drops of butyric acid.
3.       Add 1 drop of concentrated sulfuric acid,
4.         Shake tube, and place into boiling water.
5.       Remove test tube from boiling water and add 20 drops of water. Shake the tube.
6.       Smell ester by wafting the vapor towards you.

Apple:

1.       Put 6 drops of methyl alcohol in a 10-cm test tube.
2.       Wearing gloves, add 2 drops butyric acid.
3.       Add 1 drop of concentrated sulfuric acid.
4.       Shake tube and place it into boiling water.
5.       Remove test tube from boiling water and add 20 drops of water. Shake the tube.
6.       Smell ester by wafting the vapor towards you.

Results



Ester
R-OH
R-COOH
Odor
Wintergreen
Methyl Alcohol
Salicylic Acid
There‟s a hint of mint. It‟s very faint, but the scent of the ester is mostly foul.
Banana
Isoamyl Alcohol
Acetic Acid
It actually smells like banana. You really can‟t smell the other chemicals.
Strawberry
Ethyl Alcohol
Butyric Acid
It smells like strawberry. You can still smell a very small hint of the acid.
Apple
Methanol
Butyric Acid
It smells a little bit like apple. At first, you couldn‟t smell it, but after a while the scent
Grape
Methyl Alcohol
Anathrnic Acid
It smells nothing at all like grape. It smells plain foul.

Analysis of Results
 


1.  What evidence do you have that an ester was produced in each of your reactions?

The evidence that I have that an ester was produced is most of my reactions is the way the esters smell. If the products of the reactions smell sweet, than you know it is an ester. If the products of the reactions smell foul, than you know it is not an ester.

2.  What is the role of sulfuric acid in this reaction? How come it isn’t listed with the other reactants?


The role of sulfuric acid in a reaction is to work as a catalyst, which helps speed up the reaction. The reason why sulfuric acid is not listed with the other reactants is


because sulfuric acid is not a reactant, which means it‟s not part of the production. Sulfuric Acid, the catalyst, does not undergo a chemical reaction, it does not change.

3.  In your own words, describe what happens at a molecular level when an alcohol and a carboxylic acid react?


When an alcohol and a carboxylic acid react, one hydrogen from the alcohol combines with an „OH‟ from the carboxylic acid. Both the “H” and “OH” are connected to organic compounds. Therefore, parts of the functional groups of these molecules have reacted with one another and created a new molecule, called an ester. An ester has a specific functional group (“O” double bonded to another “O,” then bonded to another “O”)  that determines its smell.

Conclusion:


The GSE that my work on this lab demonstrates mastery in is Science Process Skills 2:11:5.5. In order to meet proficiency in this GSE, students will discover how the composition of a molecule affects its interactions with other molecules. In order to conduct the lab, my partners and I had to combine different types of chemicals made up of different structures, which would react, and result in an ester. For example, in order to make an ester smell like banana, we had to
combine methyl alcohol (an alcohol) and acetic acid (a carboxylic acid). The compositions of these chemicals were different, but once they we combined them and heated them up, they produced a sweet-smelling molecule. Although in class we had learned about the process, but it wasn‟t until the actual lab that I discovered and witnessed that when you combine an alcohol and a carboxylic acid (which smells putrid), you get a sweet-smelling compound. The other way my work on this lab shows proficiency in this GSE are the chemical reactions. In doing the reactions, I was able to show the way an ester looks once the alcohol and carboxylic acid react in the form of a skeletal structure.

Komentar

  1. Please conclude again about defenition of report?

    BalasHapus
    Balasan
    1. A report is a document that presents information in an organized format for a specific audience and purpose. Although summaries of reports may be delivered orally, complete reports are almost always in the form of written documents.
      Types of reports include: memos, minutes, lab reports, book reports, progress reports, justification reports, compliance reports, annual reports, and policies and procedures.

      Hapus
  2. Can you explain how we can make a best report ??

    BalasHapus
    Balasan
    1. #1 – Determine its purpose
      Before you do anything else, clearly define what your report should accomplish. Are you writing this report to persuade or inform? Will it project into the future or review the past?

      If you were assigned this report, discuss its aim with the person who put you in charge. Don’t proceed until you fully understand why you’re doing what you’re doing because everything else flows from that.

      #2 – Write to your readers
      This is really closely related to the first tip. You can’t write to your readers if you don’t know who they are. Are they experienced or inexperienced? Insiders or outsiders?

      Don’t use words, including jargon, that they won’t understand. Provide supplemental information at the end of the report if it will help. Resist the temptation to tout your horn too loudly – your report should do that for you.

      Keep your audience at the top of your mind throughout the rest of this process. You’ll look your best by looking out for your readers.

      #3 – Proceed in an orderly manner
      Now that you know why you’re writing the report, and to whom you’re reporting, you can begin doing your research. Once you’ve gathered all the information you need, you’re ready to start writing.

      When you’ve finished writing everything else, you’re ready to write your executive summary – the last thing you write will likely be the first thing your audience reads.

      #4 – Length matters
      Your report should be long enough to accomplish its purpose, but not a single word longer. Anticipate questions and objections and provide responses.

      Don’t feel the need to fill space. Don’t be redundant. Communicate effectively – end of story!

      #5 – Flow logically
      It may sound silly, but some people forget this simple rule – your report should have an introduction, the body, and a conclusion.

      It should flow easily from point-to-point. Lead the reader through a logical progression of the topic from beginning to end. Your first point should naturally flow into the second and so on.

      #6 – Appearance matters
      Your report should be visually appealing. Your readers should get a sense of what you’re saying just by scanning it. Be liberal in your use of headers and sub-headers.

      Use color if your budget permits. Present large amounts of data graphically – in a chart, a graph, a table, or some other illustration. Call out important points. Be creative, but make sure it doesn’t interfere with your message.

      #7 – Review and revise
      Once you’ve written everything, including the Executive Summary, you’re ready to review and revise your document. You should do this once and then put it away, at least overnight.

      When you come back to it, review and revise it again. Then put it away. Read through it at least one more time. You should also try to get someone else to review it for you. A fresh set of eyes will often catch mistakes that you won’t.

      Hapus
  3. In your own words, describe what happens at a molecular level when an alcohol and a carboxylic acid react?

    BalasHapus
    Balasan
    1. When an alcohol and a carboxylic acid react, one hydrogen from the alcohol combines with an „OH‟ from the carboxylic acid. Both the “H” and “OH” are connected to organic compounds. Therefore, parts of the functional groups of these molecules have reacted with one another and created a new molecule, called an ester. An ester has a specific functional group (“O” double bonded to another “O,” then bonded to another “O”) that determines its smell.

      Hapus
  4. How does the preparation of alcohols and carboxylic acids produce ester?

    BalasHapus
    Balasan
    1. Various Alcohols
      · Various Organic Acids
      · Test Tubes (5-8)
      · Hot Plate
      · Gloves
      · Goggles
      · Pipettes
      · Stirring Rods

      Hapus
  5. what is the function of sulfuric acid in your report?

    BalasHapus
    Balasan
    1. The role of sulfuric acid in a reaction is to work as a catalyst, which helps speed up the reaction. The reason why sulfuric acid is not listed with the other reactants is

      Hapus
  6. Explain what is the use of methyl alcohol in the experiment?

    BalasHapus
    Balasan
    1. we had to
      combine methyl alcohol (an alcohol) and acetic acid (a carboxylic acid). The compositions of these chemicals were different, but once they we combined them and heated them up, they produced a sweet-smelling molecule. Although in class we had learned about the process, but it wasn‟t until the actual lab that I discovered and witnessed that when you combine an alcohol and a carboxylic acid (which smells putrid), you get a sweet-smelling compound. The other way my work on this lab shows proficiency in this GSE are the chemical reactions. In doing the reactions, I was able to show the way an ester looks once the alcohol and carboxylic acid react in the form of a skeletal structure.

      Hapus
  7. What do you do so that your students like the subjects you teach?

    BalasHapus
    Balasan
    1. Make a varied method that will not make the students bored, for example take your students to a shady schoolyard and teach there or let the kids 'chat' in the classroom to relax lessons, I think it's okay for children to learn in learning

      Hapus
  8. Mention the usefulness of esters in daily life?

    BalasHapus
    Balasan

    1. 1. Esters derived from fruits are used for the aroma (essential) in food.2. Ester fat to make butter, margarine, and soap.3. Candle esters are used for cars and batik

      Hapus
  9. Whether the design in making the report always as you have explained, or may be different ie more detail or more simple?

    BalasHapus
    Balasan

    1. Not always that as I explained this could be more detailed or simpler

      Hapus
  10. What are the functional groups?

    BalasHapus
    Balasan

    1. To make things easier in grouping things

      Hapus

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